The Attempted synthesis of novel BIS(quadridentate) niobium(IV) complexes and the analyses of the products resulting from the attempted synthesis of tetrakis (8-hydroxyquinolinato) niobium (IV)

Show full item record

Title: The Attempted synthesis of novel BIS(quadridentate) niobium(IV) complexes and the analyses of the products resulting from the attempted synthesis of tetrakis (8-hydroxyquinolinato) niobium (IV)
Author: Pinkes, John R.
Abstract: Four previously reported quadridentate ligands were synthesized, and the attempts made to synthesize the corresponding bis(quadridentate)niobium( IV) complexes are documented. Attempts made to synthesize the previously reported tetrakis(bidentate) niobium ( IV) complexes of benzoyltrifluoroacetylacetone (Nb(BTA)O1 and of 8- hydroxyquinoline (Nb(8-Q)4)t are also discussed. Though neither of the desired complexes was synthesized, the resulting complexes from the attempted synthesis of the Nb(8-Q)4 complex, and their subsequent analyses, are examined in detail. Along with the ligand syntheses and the attempted coraplexations , modifications in the experimental techniques and the apparatus are also discussed .
Record URI: http://hdl.handle.net/1850/10690
Date: 1989-08-16

Files in this item

Files Size Format View
JPinkesThesis08-16-1989.pdf 13.13Mb PDF View/Open

The following license files are associated with this item:

This item appears in the following Collection(s)

Show full item record

Search RIT DML


Advanced Search

Browse